Microscopy lab services with MicroVision Laboratories? In Fourier Transform Infrared (FTIR) Spectroscopy samples are subjected to a broad frequency spectrum of infrared light which spans the energies of intramolecular vibrations, especially in organic compounds. The pattern and intensity of frequencies absorbed by a sample are plotted, which gives structural information about the chemical bonding state of the material. Organic compounds, which are generally very similar from an elemental standpoint, can be separated and identified using these structural fingerprints. See a few extra details on ftir surface analysis lab.
Analysis and Results: The submitted bottle was examined for signs of interior distress, and the water from the bottle was removed and maintained. Some of the suspended particulate was filtered and examined non-destructively by light microscopy first, to characterize the material. A low magnification stereo microscope image of the filtered white particulate is shown in the image above. From this image, biological tissues were ruled out, and the material was observed to be crystalline. Polarized light microscopy (PLM) was used to analyze the sample next. From this examination, the material showed birefringence as shown in the PLM image on the right. The PLM Image Stereo Microscope image suspect material showed optical properties and morphology dissimilar to common carbonates and sulfates. It was determined to be a birefringent crystalline material, but it could not be identified using only PLM methods. Therefore, analysis using scanning electron microscopy with energy dispersive x-ray spectroscopy (SEM-EDS) would have to be performed to obtain further information about the suspect material.
The scan from left to right shows a high tin concentration (green line) while areas of higher lead concentrations (blue line) were not intersected by the line scan. At the interface between the tin/lead solder and copper (red line), there is a mixture of the solder and copper which is the intermetallic layer. The EDS Map provides a nice visual mixture of colors which shows the intermetallic layer while the line scan clearly shows the intermetallic with the elemental graph.
What is your standard turnaround time (TAT) and can it be expedited? Our standard TAT is 5 to 10 business days. We can provide faster TATs on request with the following surcharges: – Same day to 24 hour rush is 100% surcharge – 2 day rush is 75% surcharge – 3 day rush is 50% surcharge – 4 day rush is 25% surcharge Rush requests must have prior approval otherwise we cannot guarantee turnaround times.
The data indicated that a significant portion of the dust was from the insulation in the attic. The contractor had replaced a portion of duct work running to the master bedroom. During this replacement, fiberglass insulation was knocked into the ducting. The small glass insulation fibers were spread through the AC ducts and settling out of the air throughout the house. The client was relieved to know what was causing their skin irritation and the significant dust build up. Using the results garnered from the analysis from MicroVision Labs they were able to have the contractor clean out the duct work and act to prevent further spread of the insulation fibers and properly clean up the settled dust in the house that was the cause of the homeowner’s skin irritation.
?We partner with companies in all phases of product development and sales, including R&D, manufacturing, QC, advertising and failure analysis. Our laboratory offers a highly-trained and experienced staff utilizing a powerful set of analytical tools (SEM with EDS and backscatter detectors, Bruker X-Flash elemental mapping, X-Ray imaging, Micro-FTIR spectroscopy, Micro-XRF, light microscopy, cross sectioning/precision polishing and microhardness testing). Read more info at https://microvisionlabs.com/.